HCID 59511048, compound → HCID 59511056, compound

Participants

Reaction Conditions

Reaction Steps

To a vial is added fluoroazide 17 (5.79 mmol) and 1-propynyl-2-nitroimidazole (5.79 mmol). The solution is heated at 60° C. overnight. The material is then purified on a silica gel column using EtOAc:Hex as the eluent. The material is then further purified via recrystallization using EtOAc:Hex to afford pale yellow crystals. Preparation of Compounds 5 and 21:

Provenance & Evidence