Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyrrolidine | HCID 31268 | — |
| Reactant | HCID 59285987 | HCID 59285987 | — |
| Product | HCID 25002216 | HCID 25002216 | 42% |
Reaction Steps
Pyrrolidine (0.5 mL) was added to 2-aminocarbonylamino-5-[2-(3-chloropropyloxy)phenyl]pyrrole-3-carboxamide (Compound No. 4-29, 30 mg, 0.090 mmol), the whole was sealed and stirred at 120° C. for 5 hours. This mixture was purified by silica gel column chromatography to give the target compound (14 mg) as a brown amorphous Powder (Yield 42%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07977371B2 |
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| Source dataset | uspto-grants-2011_07 |
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| ORD ID | ord-d26a0cb45c5d4237aeebcf4a586b5078 |
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| Source note | uspto-grants-2011_07 |
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