HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Diethylamino)pyrrolidine → [5-(3-Bromo-phenyl)-2,4-dimethyl-2H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Diethylamino)pyrrolidine | HCID 19961995 | — |
| Reactant | HCID 67315642 | HCID 67315642 | — |
| Product | [5-(3-Bromo-phenyl)-2,4-dimethyl-2H-pyrazol-3-yl]-(3-diethylamino-pyrrolidin-1-yl)-methanone | HCID 67314617 | 77% |
Reaction Steps
In analogy to the procedure described in example 12D), 5-(3-bromo-phenyl)-2,4-dimethyl-2H-pyrazole-3-carboxylic acid and 3-(diethylamino)pyrrolidine gave the title compound in 77% yield as light yellow viscous oil. MS: 419.0 (MH+, 1 Br).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-0acad17e62ac40d3b53f117620b02091 |
| Source note | uspto-grants-2011_07 |