HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodobenzene → HCID 178463851, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodobenzene | HCID 11575 | — |
| Reactant | (3-Diethylamino-pyrrolidin-1-yl)-[5-(3-ethynyl-phenyl)-4-methyl-1H-pyrazol-3-yl]-methanone | HCID 178436202 | — |
| Product | HCID 178463851 | HCID 178463851 | 70% |
Reaction Steps
In analogy to the procedure described in Example 31F], iodobenzene and (3-diethylamino-pyrrolidin-1-yl)-[5-(3-ethynyl-phenyl)-4-methyl-1H-pyrazol-3-yl]-methanone (Example 31E]) gave the title compound in 70% yield light yellow semisolid. MS: 427.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-c974724f9aa94715bfb25755866676f5 |
| Source note | uspto-grants-2011_07 |