HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzene, 1,2-dichloro-4-iodo- → HCID 178463854, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzene, 1,2-dichloro-4-iodo- | HCID 88591 | — |
| Reactant | (3-Diethylamino-pyrrolidin-1-yl)-[5-(3-ethynyl-phenyl)-4-methyl-1H-pyrazol-3-yl]-methanone | HCID 178436202 | — |
| Product | HCID 178463854 | HCID 178463854 | — |
Reaction Steps
In analogy to the procedure described in Example 31F], 1,2-dichloro-4-iodobenzene and (3-diethylamino-pyrrolidin-1-yl)-[5-(3-ethynyl-phenyl)-4-methyl-1H-pyrazol-3-yl]-methanone (Example 31E]) gave the title compound in 71% yield yellow foam. MS: 495.2 (MH+, 2 Cl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-af0f39b492d14fb3b39303ef6ad3d00e |
| Source note | uspto-grants-2011_07 |