HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1-Pyrrolidinyl)piperidine → HCID 57554938, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1-Pyrrolidinyl)piperidine | HCID 78703 | — |
| Reactant | HCID 67314819 | HCID 67314819 | — |
| Product | HCID 57554938 | HCID 57554938 | 27% |
Reaction Steps
In analogy to the procedure described in Example 18], 1-(2-methoxy-5-trifluoromethyl-phenyl)-3,5-dimethyl-1H-pyrazole-4-carboxylic acid and 4-pyrrolidine-1-yl-piperidine gave, after purification on a flash isolute NH2-column (EtOAc:n-heptane 4:1), the title compound in 27% yield as yellow oil. MS: 451.2 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-704e06e760414a39a926824331f1cf53 |
| Source note | uspto-grants-2011_07 |