HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-acetylacetoacetate → HCID 67314600, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-acetylacetoacetate | HCID 79063 | — |
| Reactant | HCID 21552091 | HCID 21552091 | — |
| Product | HCID 67314600 | HCID 67314600 | 96% |
Reaction Steps
In analogy to the procedure described in Example 38A], (4-methyl-3-trifluoromethyl-phenyl)-hydrazine and ethyl diacetoacetate gave the title compound after crystallisation (EtOAc) in 96% yield as red oil. MS: 327.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-128647d89de04a83b862e5b0e8aafed2 |
| Source note | uspto-grants-2011_07 |