HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) → HCID 67314818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-(Trifluoromethoxy)phenylboronic Acid (contains varying amounts of Anhydride) | HCID 2734385 | — |
| Reactant | HCID 178469165 | HCID 178469165 | — |
| Product | HCID 67314818 | HCID 67314818 | 54% |
Reaction Steps
In analogy to the procedure described in Example 160C], 5-cyclopropyl-3-(1,3-dioxo-1,3-dihydro-isoindol-2-ylmethyl)-1H-pyrazole-4-carboxylic acid ethyl ester and 3-(trifluoromethoxy)benzeneboronic acid gave the title compound as a white solid (54%). MS: 500.0 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-99b5a588521e4503a98830cdd0d14da9 |
| Source note | uspto-grants-2011_07 |