HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67314549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 86626596 | HCID 86626596 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67314549 | HCID 67314549 | 84% |
Reaction Steps
Treatment of (trans) 2-methyl-4-pyrrolidin-1-yl-piperidine-1-carboxylic acid tert-butyl ester (0.1 g, 0.4 mmol) with 4M hydrochloric acid in dioxane (5 ml) for 1 h and subsequent evaporation of the solvent afforded the title compound (0.06 g, 84%) as a white powder. MS: 169.1 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-8d8a967eea7e40649871b86188cbfa17 |
| Source note | uspto-grants-2011_07 |