HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67315126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Reactant | 1′-(1,1-Dimethylethyl) 5′-methyl [1,3′-bipyrrolidine]-1′,5′-dicarboxylate | HCID 69817351 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67315126 | HCID 67315126 | — |
Reaction Steps
The title compound was prepared in analogy to 193B, by reduction of 3′S,5′S)-[1,3′]Bipyrrolidinyl-1′,5′-dicarboxylic acid 1′-tert-butyl ester 5′-methyl ester with lithium aluminium hydride and subsequent deprotection with 4M hydrochloric acid in dioxane. MS: 171.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977358B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-5cddac67714a401a9b26586084fd352a |
| Source note | uspto-grants-2011_07 |