反应详情

To 40 mg of 2-mercapto-5-nitropyridine was added 200 mL of acetone, and the solution was stirred while cooled with water. To this reaction solution were added 43.6 of 4-chloromethylbenzaldehyde and 45 g of potassium carbonate, to conduct reaction. After the completion of the reaction, 1 L of water was added to the solution. The precipitated crystal was collected by filtration, washed with water, washed with methanol, and dried (yield amount 65.5 g, and yield 93.3%).

1. customreaction
2. additionwas added to the solution
3. filtrationThe precipitated crystal was collected by filtration
4. washwashed with water
5. washwashed with methanol
6. customdried
7. custom(yield amount 65.5 g, and yield 93.3%)