Sodium borohydride → HCID 67315794, compound

Participants

Reaction Steps

560 mg (1.46 mmol, 1.0 equivalent) of {(4-dipropylaminobutyl)-[4-(1H-imidazol-2-ylmethylidene)aminomethylbenzyl]methyl}amine (43) and 12 ml of methanol were charged in a 50 ml recovery flask under a nitrogen stream. The mixture was then stirred. 113 mg (2.92 mol, 2.0 equivalents) of sodium borohydride was added to the mixture at 0° C. The mixture was then stirred at 0° C. for one hour and at 20° C. for one hour.

Provenance & Evidence