HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67313368, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 58677612 | HCID 58677612 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67313368 | HCID 67313368 | — |
Reaction Steps
Compound 298 (0.57 g, 1.14 mmol) was dissolved in CH2Cl2 (10 mL) and CF3COOH (10 mL) was added. The reaction mixture was stirred at room temperature for 2 h after which the solvent was concentrated. The solid was recrystallized from CH2Cl2. This gave the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07977387B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-d3b24bcccea84f30ac142758eebf68c0 |
| Source note | uspto-grants-2011_07 |