HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzothiazole → HCID 178424116, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzothiazole | HCID 18272 | — |
| Reactant | 3-Oxo-3,4-dihydro-2H-1,4-benzothiazine-6-carbaldehyde | HCID 10943348 | — |
| Reactant | HCID 178502731 | HCID 178502731 | — |
| Product | HCID 178424116 | HCID 178424116 | — |
Reaction Steps
Using 4-methyl-benzothiazole (5 mmol, obtained by reductive deamination of 2-amino-4-methylbenzothiazole), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 3-oxo-3,4-dihydro-2H-benzo[1,4]thiazine-6-carbaldehyde (0.3 mmol) in according to the same protocol as that described for example 1, steps 1.a to 1.c, the title compound was obtained as a yellowish solid (55 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981886B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-8aa29d126a014d658f2c4e421899a594 |
| Source note | uspto-grants-2011_07 |