HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzo(B)Thiophene → HCID 178519276, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzo(B)Thiophene | HCID 7221 | — |
| Reactant | 2,3-Dihydro-1,4-benzodioxin-6-carbaldehyde | HCID 248127 | — |
| Reactant | HCID 178502731 | HCID 178502731 | — |
| Product | HCID 178519276 | HCID 178519276 | — |
Reaction Steps
Using thianaphthene (5 mmol), [trans-4-(methoxy-methyl-carbamoyl)-cyclohexyl]-carbamic acid tert-butyl ester (2.5 mmol) and 2,3-dihydro-benzo[1,4]dioxine-6-carbaldehyde (0.4 mmol) according to the same protocol as that described for example 1, steps 1.a to 1.c, the title compound was obtained as a colourless oil which solidified on standing (50 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981886B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-dd7ee9b612184208bff09b3f7f6ea380 |
| Source note | uspto-grants-2011_07 |