HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(Thiophen-3-yl)ethanone → HCID 5373947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(Thiophen-3-yl)ethanone | HCID 15116 | — |
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Product | HCID 5373947 | HCID 5373947 | 70.1% |
Reaction Steps
Stir 1-thien-3-ylethanone (1.26 g, 10 mmol) with N,N-dimethylformamide dimethyl acetal (2.66 mL, 20 mmol) at reflux for 4 h. Cool to RT, concentrate and dry in a vacuum oven to give the title compound as a brown solid (1.27 g, 70%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981882B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-dc71ff4a4034483494dba1dce70d4903 |
| Source note | uspto-grants-2011_07 |