HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → HCID 16004699, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | HCID 16004700 | HCID 16004700 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 16004699 | HCID 16004699 | 78.4% |
Reaction Steps
Add succinic acid (55.9 mg, 0.47 mmol) to a solution of 7-chloro-6-(3,5-dimethylpyrazol-1-yl)-2,3,4,5-tetrahydro-1H-benzo[d]azepine (130.5 mg, 0.47 mmol) in methanol (3 mL). Stir the reaction at RT for 15 min, and concentrate to give the title compound (145.19 mg, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981882B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-abf78bd9315844cba8252b20c8c730bb |
| Source note | uspto-grants-2011_07 |