Succinic Acid → HCID 67318095, compound

Participants

Reaction Steps

Dissolve 6-(azetidin-1-yl)-7-chloro-2,3,4,5-tetrahydro-1H-benzo[d]azepine (63 mg, 0.27 mmol) in methanol (1 mL). Add one equivalent of succinic acid (31 mg, 0.27 mmol) in methanol (1 mL) stir, concentrate to an oil, add anhydrous diethyl ether to precipitate out the solid. Decant the solvent and dry the solid under a stream of nitrogen to give the title compound as a solid.

Provenance & Evidence