Hydrochloric Acid → HCID 59789454, compound

HRID 1013349Notes

Reaction equation

HRID 1013349 reaction equation
Cl.C(OC([N:9]1[CH2:22][CH:12]2[C:13]3[C:14]([C:20]#[N:21])=[C:15]([Cl:19])[S:16][C:17]=3[CH2:18][CH:11]2[CH2:10]1)=O)(C)(C)C>>[Cl:19][C:15]1[S:16][C:17]2[CH2:18][CH:11]3[CH2:10][NH:9][CH2:22][CH:12]3[C:13]=2[C:14]=1[C:20]#[N:21]

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 131727021HCID 131727021, compound

Product 1

HCID 59789454HCID 59789454, compound

Procedure

The title compound was prepared as its HCl salt by the method of Example 1, step b) utilizing the product of step d). 1H NMR (300 MHz, CDCl3, ppm) 2.75-2.82 (m, 1H); 2.92-3.05 (m, 1H); 3.12-3.45 (m, 4H); 3.50-3.62 (m, 1H); 3.82-3.95 (m, 1H); 7.10-7.30 (br s, 2H); MS calculated for C10H9ClN2S +H 225, observed 225.

Sources & evidence

ORD record
ord-00d2bcb6b95b428aa7a05698b5093b22
Source dataset
uspto-grants-2011_07
Patent number
US07981919B2

Reaction notes

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