HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131729025, compound → HCID 59789449, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131729025 | HCID 131729025 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 59789449 | HCID 59789449 | — |
Reaction Steps
The product of step b) was dissolved in EtOAc (50 ml) and 10% Pd/C (1 gram) was added. The flask was evacuated and purged four times with N2 and then a balloon of H2 was added and the reaction was stirred for 24 hours at room temperature. Next, the mixture was passed through a pad of celite and the solvent was concentrated providing the subtitled product that was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981919B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-eeadfd946288456baebf5ab8c718dbae |
| Source note | uspto-grants-2011_07 |