HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67207770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67207033 | HCID 67207033 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67207770 | HCID 67207770 | — |
Reaction Steps
The product from step b) (2.0 g, 0.0077 mol) was dissolved in 20 mL dichloromethane and was treated with 10 mL of TFA and stirred for 2 hours at room temperature. The solvent was evaporated in vacuo to give the crude subtitle compound that was used in the next step without further purification. MS calculated for C21H21NO2S +H: 352, observed: 352.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07981919B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-0d6ed1d22f4f4f5282f66526ea180c95 |
| Source note | uspto-grants-2011_07 |