Hydrochloric Acid → HCID 57925869, compound

Participants

Reaction Steps

Methyl 4-[(dimethoxyphosphoryl)amino]benzoate (1.50 g, 5.79 mmol) was made 0.25 M in dioxane and to this stirring solution was added 3M aq LiOH. The resulting solution was stirred at ambient temperature for 16 h. The reaction mixture was then neutralized to pH=7 with 1N aq HCl and concentrated in vacuo to afford the requisite product. MS: cal'd 243 (MH+), exp 243 (MH+)

Provenance & Evidence