(4,5,6,7-Tetrahydro-1H-indazol-4-yl)-carbamic acid benzyl ester → 4,5,6,7-tetrahydro-1H-indazol-4-amine

Beteiligte Stoffe

Reaktionsschritte

Stir a mixture of (4,5,6,7-tetrahydro-1H-indazol-4-yl)-carbamic acid benzyl ester (3.5 g) methanol (50 mL) and palladium on carbon (10%, 0.7 g) on a hydrogenation parr shaker under 50 psi for 3 hours. Remove the reaction from parr shaker and filter the mixture through celite. Concentrate the filtrate to afford 1.7 g of the title compound.

Herkunft & Nachweise