HRID1013815

反应详情

EQUATION

反应方程式

HRID 1013815 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Stir a mixture of (4,5,6,7-tetrahydro-1H-indazol-4-yl)-carbamic acid benzyl ester (3.5 g) methanol (50 mL) and palladium on carbon (10%, 0.7 g) on a hydrogenation parr shaker under 50 psi for 3 hours. Remove the reaction from parr shaker and filter the mixture through celite. Concentrate the filtrate to afford 1.7 g of the title compound.

WORKUP

后处理

  1. customRemove
  2. customthe reaction from parr shaker
  3. filtrationfilter the mixture through celite
  4. concentrationConcentrate the filtrate