1-Iodopropane → HCID 67317167, compound

Participants

Reaction Conditions

Reaction Steps

To pinacolone (50 mL, Aldrich) was added 3-[4-(methyloxy)-3-nitrophenyl]pyridine (3.5 g, 15.22 mmol) and propyliodide (10.46 g, 61.52 mmol, Fluke). The reaction was stirred at 95° C. overnight. The solvent was decanted and the remaining solids were dried under reduced pressure overnight to provide 3-[4-(methyloxy)-3-nitrophenyl]-1-propylpyridinium iodide, which was use for the next reaction without further purification.

Provenance & Evidence