HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 67316482, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 3-[(2-Methoxybenzyl)oxy]benzaldehyde | HCID 19744674 | — |
| Product | HCID 67316482 | HCID 67316482 | — |
Reaction Steps
Addition of acetonitrile to 3-(2-methoxybenzyloxy)benzaldehyde gave 3-(3-(2-methoxybenzyloxy)phenyl)-3-hydroxypropanenitrile as yellow oil. Yield (0.88 g, 47%): NMR (400 MHz, CDCl3) δ 7.42-7.46 (m, 1H), 7.27-7.31 (m, 2H), 6.90-7.06 (m, 5H), 5.12 (s, 2H), 5.01 (m, 1H), 3.87 (s, 3H), 2.76-2.82 (m, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07982071B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-692aea7b6c9a4367a749c2ed838ddc57 |
| Source note | uspto-grants-2011_07 |