Isopropanol → HCID 178457226, compound

HRID 1014912Notes

Reaction equation

HRID 1014912 reaction equation
[C:1]([S:14]([N:17]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][C:26]([O:28]CC)=[O:27])[CH2:18][CH2:19][CH3:20])(=[O:16])=[O:15])([C:4]([C:7]([C:10]([F:13])([F:12])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2].[OH-].[K+:32].C(O)(C)C>O>[C:1]([S:14]([N:17]([CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][C:26]([O:28][K:32])=[O:27])[CH2:18][CH2:19][CH3:20])(=[O:16])=[O:15])([C:4]([C:7]([C:10]([F:13])([F:12])[F:11])([F:9])[F:8])([F:6])[F:5])([F:3])[F:2]

Participants

5

Reactant 3

HCID 3776IsopropanolHCID 14797Potassium HydroxideHCID 131726676HCID 131726676, compound

Product 1

HCID 178457226HCID 178457226, compoundYield 61.3%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A round bottom flask fitted with an overhead stirrer was charged with C4F9SO2N(C3H7)(CH2)5COOC2H5 (63.0 g; 0.143 mole), KOH (13.1 g; 0.234 mole; pellets) isopropanol (26 mL) and deionized water (21 mL). The ensuing mixture was refluxed overnight, cooled to room temperature, yielding a solution of C4F9SO2N(C3H7)(CH2)5COOK (61.3% solids).

Workup

  1. customA round bottom flask fitted with an overhead stirrer
  2. temperatureThe ensuing mixture was refluxed overnight

Sources & evidence

ORD record
ord-ad45df2131974a05bc98fc549158b15c
Source dataset
uspto-grants-2011_07
Patent number
US07985723B2

Reaction notes

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