Nitromethane → 1-(2-Nitro-vinyl)-4-trifluoromethyl-benzene

HRID 1014999Notes

Reaction equation

[F:1][C:2]([F:12])([F:11])[C:3]1[CH:10]=[CH:9][C:6]([CH:7]=O)=[CH:5][CH:4]=1.[N+:13]([CH3:16])([O-:15])=[O:14]>>[N+:13]([CH:16]=[CH:7][C:6]1[CH:9]=[CH:10][C:3]([C:2]([F:12])([F:11])[F:1])=[CH:4][CH:5]=1)([O-:15])=[O:14]

Participants

Reactant 2

HCID 6375Nitromethane

HCID 679964-(Trifluoromethyl)benzaldehyde

Product 1

HCID 6882311-(2-Nitro-vinyl)-4-trifluoromethyl-benzeneYield 98%

Procedure

In close analogy to the procedure described above, 4-Trifluoromethyl-benzaldehyde is reacted with nitromethane to provide the title compound.

Sources & evidence

ORD record: ord-75085dee46d64ff793a6275e6f305d02
Source dataset: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07985753B2

Reaction notes

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