Sodium triacetoxyborohydride → 1176414-95-1

HRID 1015058Notes

Reaction equation

[Br:1][C:2]1[CH:11]=[C:10]2[C:5]([CH2:6][CH2:7][N:8]=[C:9]2[CH3:12])=[CH:4][CH:3]=1.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[Br:1][C:2]1[CH:11]=[C:10]2[C:5]([CH2:6][CH2:7][NH:8][CH:9]2[CH3:12])=[CH:4][CH:3]=1

Participants

Reactant 2

HCID 5049666Sodium triacetoxyborohydride

HCID 186801367-Bromo-1-methyl-3,4-dihydroisoquinoline

Product 1

HCID 584164221176414-95-1

Procedure

In close analogy to the procedure described above, 7-bromo-1-methyl-3,4-dihydro-isoquinoline is reacted with sodium triacetoxyborohydride to provide the title compound.

Sources & evidence

ORD record: ord-439abe1b4de44ef091da2e07c7074a6b
Source dataset: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07985753B2

Reaction notes

Loading…