Sodium triacetoxyborohydride → HCID 58416480, compound

HRID 1015064Notes

Reaction equation

[CH3:1][C:2]1[C:3]2[C:8]([CH2:9][CH2:10][N:11]=1)=[C:7]1[O:12][CH2:13][O:14][C:6]1=[CH:5][CH:4]=2.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[CH3:1][CH:2]1[NH:11][CH2:10][CH2:9][C:8]2[C:3]1=[CH:4][CH:5]=[C:6]1[O:14][CH2:13][O:12][C:7]1=2

Participants

Reactant 2

HCID 5049666Sodium triacetoxyborohydride

HCID 58416494HCID 58416494, compound

Product 1

HCID 58416480HCID 58416480, compound

Procedure

In close analogy to the procedure described above, 6-Methyl-8,9-dihydro-1,3-dioxa-7-aza-cyclopenta[a]naphthalene is reacted with sodium triacetoxyborohydride to provide the title compound.

Sources & evidence

ORD record: ord-c27c9599d20a4712ac294d24b6846d57
Source dataset: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07985753B2

Reaction notes

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