Sodium triacetoxyborohydride → HCID 59662591, compound

HRID 1015065Notes

Reaction equation

[CH3:1][C:2]1[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[O:11][CH2:10][CH2:9][O:8]3)[CH2:5][CH2:4][N:3]=1.C(O[BH-](OC(=O)C)OC(=O)C)(=O)C.[Na+]>>[CH3:1][CH:2]1[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[O:11][CH2:10][CH2:9][O:8]3)[CH2:5][CH2:4][NH:3]1

Participants

Reactant 2

HCID 5049666Sodium triacetoxyborohydride

HCID 58416302HCID 58416302, compound

Product 1

HCID 59662591HCID 59662591, compound

Procedure

In close analogy to the procedure described above, 8-methyl-2,3,5,6-tetrahydro-1,4-dioxa-7-aza-phenanthrene is reacted with sodium triacetoxyborohydride to provide the title compound.

Sources & evidence

ORD record: ord-c547519cc207494699235b6afd36960e
Source dataset: uspto-grants-2011_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07985753B2

Reaction notes

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