Aluminium lithium hydride → HCID 67302009, compound

Participants

Reaction Steps

4-(2,6-Difluorophenoxy)cyclohexanecarboxylic acid ethyl ester (155 mg, 0.55 mmol) was carried out using Method H with lithium aluminum hydride (150 mg; 3.95 mmol) in tetrahydrofuran at 0° C. under nitrogen flow. Material was purified by flash chromatography using 2% methanol in dichloromethane to give 109 mgs of title compound. (82% yield).

Provenance & Evidence