HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylsilane → HCID 67301422, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 178525725 | HCID 178525725 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 67301422 | HCID 67301422 | 42% |
Reaction Steps
Trans-4-(2-chlorobenzoyl)cyclohexane-1-carboxylic acid (300 mg; 1.12 mmol) and triethylsilane (654 mg; 5.62 mmol) was carried out using Method G in 4 mL of trifluoroacetic acid. Title compound was obtained as a white solid. (118 mg; 42% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07985755B2 |
| Source dataset | uspto-grants-2011_07 |
| ORD ID | ord-e91b5f9ac8294aeab6790cbd5d92165c |
| Source note | uspto-grants-2011_07 |