Aluminium lithium hydride → HCID 67301499, compound

Participants

Reaction Steps

4-(2-Chlorobenzyl)cyclohexanecarboxylic acid (115 mg; 0.48 mmol) and lithium aluminum hydride (100 mg; 2.64 mmol) was carried out using Method H in 5 mL tetrahydrofuran. Material was purified by flash chromatography using 10-50% ethyl acetate in hexanes gradient to give 73 mgs of title compound. (67% yield).

Provenance & Evidence