2-Methoxyethylamine → HCID 24772473, compound

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Reaction Steps

The title compound was prepared from the product of Example 45A and 2-methoxyethylamine using the procedure described for Example 2B. 1H NMR (DMSO-d6, 300 MHz) δ 1.45 (s, 6H), 1.48 (s, 6H), 3.18 (s, 3H), 3.31-3.41 (m, 4H), 7.68-7.82 (m, 3H), 7.99 (t, J=5.3 Hz, 1H), 11.51 (br s, 1H). MS (ESI+) m/z 489 (M+H)+. Anal. calcd. for C22H24F4N2O4S: C, 54.09; H, 4.95; N, 5.73. Found: C, 53.88; H, 4.65; N, 5.71.

Provenance & Evidence