Ethanolamine → HCID 24772744, compound

Participants

Reaction Steps

The title compound was prepared from the product of Example 45A and commercially available 2-hydroxyethylamine using the procedure described for Example 2B. 1H NMR (DMSO-d6, 300 MHz) δ 1.45 (s, 6H), 1.48 (s, 6H), 3.24 (q, J=6.2 Hz, 2H), 3.43 (q, J=5.6 Hz, 2H), 4.65 (t, J=5.6 Hz, 1H), 7.68-7.81 (m, 3H), 7.89 (t, J=5.6 Hz, 1H), 11.58 (br s, 1H). MS (ESI+) m/z 475 (M+H)+.

Provenance & Evidence