Resorcinol → HCID 57889822, compound

HRID 1016131Notes

Reaction equation

HRID 1016131 reaction equation
O[C:2]1[CH:3]=[C:4]([OH:8])[CH:5]=[CH:6][CH:7]=1.Br[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=1[NH:16][C:17]([NH2:19])=[O:18]>>[OH:8][C:4]1[CH:3]=[C:2]([C:10]2[CH:15]=[CH:14][CH:13]=[CH:12][C:11]=2[NH:16][C:17]([NH2:19])=[O:18])[CH:7]=[CH:6][CH:5]=1

Participants

3

Reactant 2

HCID 5054ResorcinolHCID 139386(2-Bromophenyl)urea

Product 1

HCID 57889822HCID 57889822, compound

Procedure

3-Hydroxy phenol and 2-bromophenyl urea were reacted under Suzuki cross coupling conditions in a similar manner as described for the preparation of Example 294 to provide 1-(3′-hydroxybiphenyl-2-yl)urea.

Workup

  1. customas described for the preparation of Example 294

Sources & evidence

ORD record
ord-953a2aec33994887831c87f18430bc59
Source dataset
uspto-grants-2011_07
Patent number
US07985861B2

Reaction notes

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