Benzaldehyde → HCID 9886906, compound

HRID 1016293Notes

Reaction equation

HRID 1016293 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:13]3=[C:14]([C:16](=[O:26])[C:17]([CH2:19][C:20]4[CH:21]=N[CH:23]=[CH:24][CH:25]=4)=[CH:18][N:12]3[C:11]3[CH:10]=[CH:9][C:8]([Cl:27])=[CH:7][C:6]=3[O:5]2)[CH:15]=1.[CH:28](=O)C1C=CC=CC=1>>[Cl:27][C:8]1[CH:7]=[C:6]2[C:11]3=[C:10]([C:16](=[O:26])[C:17]([CH2:19][C:20]4[CH:21]=[CH:28][CH:23]=[CH:24][CH:25]=4)=[CH:18][N:12]3[C:13]3[CH:14]=[CH:15][C:2]([Cl:1])=[CH:3][C:4]=3[O:5]2)[CH:9]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 9908665HCID 9908665, compound

Product 1

HCID 9886906HCID 9886906, compoundYield 81%

Procedure

According to Example 1<step 4>, the compound (500 mg) produced in Example 1<step 3> was reacted with benzaldehyde (260 μl) to obtain the title compound (508 mg; 81%).

Sources & evidence

ORD record
ord-8cd03a0927534fdfb8aa0a185d8248da
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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