Benzaldehyde → HCID 18406584, compound

HRID 1016295Notes

Reaction equation

HRID 1016295 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]2[C:13]3=[C:14]([C:16](=[O:26])[C:17]([CH2:19][C:20]4[CH:21]=N[CH:23]=[CH:24][CH:25]=4)=[CH:18][N:12]3[C:11]3[CH:10]=[CH:9][C:8]([Cl:27])=[CH:7][C:6]=3[S:5]2)[CH:15]=1.[CH:28](=O)C1C=CC=CC=1>>[CH2:19]([C:17]1[C:16](=[O:26])[C:14]2[CH:15]=[C:2]([Cl:1])[CH:3]=[C:4]3[C:13]=2[N:12]([CH:18]=1)[C:11]1[CH:10]=[CH:9][C:8]([Cl:27])=[CH:7][C:6]=1[S:5]3)[C:20]1[CH:21]=[CH:28][CH:23]=[CH:24][CH:25]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 18406533HCID 18406533, compound

Product 1

HCID 18406584HCID 18406584, compoundYield 60%

Procedure

According to Example 1<step 4>, the compound (30 mg) produced in Example 5<step 3 >was reacted with benzaldehyde (15 μl) to obtain the title compound (23 mg; 60%).

Sources & evidence

ORD record
ord-0ed945822fa84c9497974d6df9339417
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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