Benzaldehyde → HCID 9907189, compound

HRID 1016297Notes

Reaction equation

[C:1]([N:4]1[C:17]2[C:12]3=[C:13]([C:18](=[O:28])[C:19]([CH2:21][C:22]4[CH:23]=N[CH:25]=[CH:26][CH:27]=4)=[CH:20][N:11]3[C:10]3[CH:9]=[CH:8][CH:7]=[CH:6][C:5]1=3)[CH:14]=[CH:15][CH:16]=2)(=[O:3])[CH3:2].[CH:29](=O)C1C=CC=CC=1>>[C:1]([N:4]1[C:17]2[C:12]3=[C:13]([C:18](=[O:28])[C:19]([CH2:21][C:22]4[CH:23]=[CH:29][CH:25]=[CH:26][CH:27]=4)=[CH:20][N:11]3[C:10]3[CH:9]=[CH:8][CH:7]=[CH:6][C:5]1=3)[CH:14]=[CH:15][CH:16]=2)(=[O:3])[CH3:2]

Participants

Reactant 2

HCID 240Benzaldehyde

HCID 12021087HCID 12021087, compound

Product 1

HCID 9907189HCID 9907189, compoundYield 36%

Procedure

According to Example 9<step 4>, the compound (5 g) produced in Example 9<step 3>was reacted with benzaldehyde (3 mL) to obtain the title compound (2.4 g; 36%).

Sources & evidence

ORD record: ord-5454205ca1b74ea2880f0c756b5e5bee
Source dataset: uspto-grants-2002_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06476021B1

Reaction notes

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