Benzaldehyde → HCID 12021091, compound

HRID 1016299Notes

Reaction equation

HRID 1016299 reaction equation
[CH3:1][N:2]1[C:15]2[C:10]3=[C:11]([C:16](=[O:26])[C:17]([CH2:19][C:20]4[CH:21]=N[CH:23]=[CH:24][CH:25]=4)=[CH:18][N:9]3[C:8]3[CH:7]=[CH:6][CH:5]=[CH:4][C:3]1=3)[CH:12]=[CH:13][CH:14]=2.[CH:27](=O)C1C=CC=CC=1>>[CH2:19]([C:17]1[C:16](=[O:26])[C:11]2[CH:12]=[CH:13][CH:14]=[C:15]3[C:10]=2[N:9]([CH:18]=1)[C:8]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[N:2]3[CH3:1])[C:20]1[CH:21]=[CH:27][CH:23]=[CH:24][CH:25]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 12021090HCID 12021090, compound

Product 1

HCID 12021091HCID 12021091, compoundYield 30%

Procedure

According to Example 1<step 4>, the compound (200 mg) produced in Example 15<step 3> was reacted with benzaldehyde (0.13 mL) to obtain the title compound (102 mg; 30%).

Sources & evidence

ORD record
ord-1c41a24c4c7c45f19dd4f8f8b0b06e50
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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