Benzaldehyde → HCID 12021093, compound

HRID 1016301Notes

Reaction equation

HRID 1016301 reaction equation
N1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:8]2[C:9](=[O:26])[C:10]3[CH:11]=[CH:12][CH:13]=[C:14]4[C:23]=3[N:22]([CH:24]=2)[C:21]2[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=2[C:15]4=[O:25])[CH:2]=1.[CH:27](=O)C1C=CC=CC=1>>[CH2:7]([C:8]1[C:9](=[O:26])[C:20]2[CH:19]=[CH:18][CH:17]=[C:16]3[C:21]=2[N:22]([CH:24]=1)[C:23]1[CH:10]=[CH:11][CH:12]=[CH:13][C:14]=1[C:15]3=[O:25])[C:3]1[CH:2]=[CH:27][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 12021092HCID 12021092, compound

Product 1

HCID 12021093HCID 12021093, compoundYield 72%

Procedure

According to Example 1<step 4>, the compound (200 mg) obtained in Example 18<step 2>was reacted with benzaldehyde (0.13 mL) to obtain the title compound (194 mg; 72%).

Sources & evidence

ORD record
ord-0c433d4ef0d54aa2ba2999017fedd8e5
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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