HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acrylate → HCID 12021094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acrylate | HCID 8821 | — |
| Reactant | HCID 18406573 | HCID 18406573 | — |
| Reactant | HCID 18406586 | HCID 18406586 | — |
| Product | HCID 12021094 | HCID 12021094 | 47% |
Reaction Steps
According to Example 5<step 1>, 8-chloro-4-cyano-5H-pyrido[4,3-b]indole (1.26 g) prepared from 5-chloro-2-cyanomethylindole by the procedure described in literature (Synthesis, 743 (1992) and Chem. Pharm. Bull., 29, 1280 (1981)) was reacted with ethyl acrylate (1.8 mL) to obtain the title compound (850 mg; 47%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476021B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-7704628f8dca4e07a003191826c7ffa7 |
| Source note | uspto-grants-2002_11 |