Benzaldehyde → HCID 9819529, compound

HRID 1016303Notes

Reaction equation

HRID 1016303 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]2[N:8]3[CH:17]=[C:16]([CH2:18][C:19]4[CH:20]=N[CH:22]=[CH:23][CH:24]=4)[C:15](=[O:25])[C:14]4[C:9]3=[C:10]([CH:11]=[CH:12][N:13]=4)[C:4]=2[CH:3]=1.[CH:26](=O)C1C=CC=CC=1>>[CH2:18]([C:16]1[C:15](=[O:25])[C:14]2[C:9]3=[C:10]([C:4]4[CH:3]=[C:2]([Cl:1])[CH:7]=[CH:6][C:5]=4[N:8]3[CH:17]=1)[CH:11]=[CH:12][N:13]=2)[C:19]1[CH:24]=[CH:23][CH:22]=[CH:26][CH:20]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 9798283HCID 9798283, compound

Product 1

HCID 9819529HCID 9819529, compoundYield 21.6%

Procedure

According to Example 1<step 4>, the compound (200 mg) produced in Example 23<step 4> was reacted with benzaldehyde (132 mg) to obtain the title compound (43 mg; 16%).

Sources & evidence

ORD record
ord-231622dc53754ecbb9c061ed00512e15
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

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