Benzaldehyde → HCID 12021096, compound

HRID 1016304Notes

Reaction equation

HRID 1016304 reaction equation
N1[CH:6]=[CH:5][CH:4]=[C:3]([CH2:7][C:8]2[C:17](=[O:18])[C:16]3[C:11]4=[C:12]([C:19]5[CH:20]=[CH:21][CH:22]=[CH:23][C:24]=5[N:10]4[CH:9]=2)[CH:13]=[CH:14][N:15]=3)[CH:2]=1.[CH:25](=O)C1C=CC=CC=1>>[CH2:7]([C:8]1[C:17](=[O:18])[C:16]2[C:11]3=[C:12]([C:19]4[CH:20]=[CH:21][CH:22]=[CH:23][C:24]=4[N:10]3[CH:9]=1)[CH:13]=[CH:14][N:15]=2)[C:3]1[CH:2]=[CH:25][CH:6]=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 240BenzaldehydeHCID 12021095HCID 12021095, compound

Product 1

HCID 12021096HCID 12021096, compoundYield 58.2%

Procedure

According to Example 1<step 4>, the compound (200 mg) produced in Example 26<step 2> was reacted with benzaldehyde (153 mg) to obtain the title compound (116 mg; 42%).

Sources & evidence

ORD record
ord-699d2978ed3d4578a9afdf6b23380c04
Source dataset
uspto-grants-2002_11
Patent number
US06476021B1

Reaction notes

Loading…