HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Chloride → 10-bromo-5-benzyloxy-2-(3-pyridylmethyl)-3H-pyrido[3,2,1-kl]phenothiazin-3-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Chloride | HCID 7503 | — |
| Reactant | 10-bromo-5-hydroxy-2-(3-pyridylmethyl)-3H-pyrido[3,2,1-kl]phenothiazin-3-one | HCID 12021105 | — |
| Product | 10-bromo-5-benzyloxy-2-(3-pyridylmethyl)-3H-pyrido[3,2,1-kl]phenothiazin-3-one | HCID 12021112 | 48% |
Reaction Steps
According to Example 34, the compound (100 mg) produced in Example 37 was reacted with benzyl chloride (39 μl) to obtain the title compound (58 mg; 48%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476021B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-b713a2b4b297468c85b6cff66a7829b9 |
| Source note | uspto-grants-2002_11 |