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HRID1016316

反应详情

EQUATION

反应方程式

HRID 1016316 的结构方程式

REACTANTS

反应物

2
结构：CN1CCCC1CCCl.Cl
HCID3017050

2-(2-Chloroethyl)-1-methylpyrrolidine--hydrogen chloride (1/1)

C7H15Cl2N

结构：O=c1c(Cc2cccnc2)cn2c3c(cc(O)cc13)Sc1ccc(Br)cc1-2
HCID12021105

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCCC(Oc2cc3c4c(c2)c(=O)c(Cc2cccnc2)cn4-c2cc(Br)ccc2S3)CC1
HCID18406591

未命名化合物

收率 37%

PROCEDURE

实验过程

According to Example 34, the compound (100 mg) produced in Example 37 was reacted with 2-(2-chloroethyl)-1-methylpyrrolidine hydrochloride (54 mg) to obtain the ring expanding title compound (46 mg; 37%).

WORKUP

后处理

  1. customto obtain the ring