Benzaldehyde → HCID 18406507, compound

HRID 1016325Notes

Reaction equation

[Br:1][C:2]1[CH:15]=[CH:14][C:13]2[S:12][C:11]3[C:6]4=[C:7]([C:18](=[O:28])[C:19]([CH2:21][C:22]5[CH:23]=N[CH:25]=[CH:26][CH:27]=5)=[CH:20][N:5]4[C:4]=2[CH:3]=1)[CH:8]=[C:9]([O:16][CH3:17])[CH:10]=3.[CH:29](=O)C1C=CC=CC=1>>[CH2:21]([C:19]1[C:18](=[O:28])[C:7]2[CH:8]=[C:9]([O:16][CH3:17])[CH:10]=[C:11]3[C:6]=2[N:5]([CH:20]=1)[C:4]1[CH:3]=[C:2]([Br:1])[CH:15]=[CH:14][C:13]=1[S:12]3)[C:22]1[CH:27]=[CH:26][CH:25]=[CH:29][CH:23]=1

Participants

Reactant 2

HCID 240Benzaldehyde

HCID 12021104HCID 12021104, compound

Product 1

HCID 18406507HCID 18406507, compoundYield 46%

Procedure

According to Example 1 <step 4>, the compound (3 g) produced in Example 36 <step 2> was reacted with benzaldehyde (1.25 mL) to obtain the title compound (1.73 g; 46%).

Sources & evidence

ORD record: ord-6c0ce69e3a4f4269aea358feaa4895ea
Source dataset: uspto-grants-2002_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06476021B1

Reaction notes

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