Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 1-Nonyl-3-(nonylamino)pyrrolidine-2,5-dione
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Nonylamine | HCID 16215 | — |
| 반응물 | N-Nonylmaleimide | HCID 512831 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 1-Nonyl-3-(nonylamino)pyrrolidine-2,5-dione | HCID 512837 | — |
반응 단계
A mixture of N-nonyl maleimide (0.01 M) prepared as described in Example 12 above, nonylamine (0.01 M), triethylamine [catalytic, 0.1 equivalent] in acetonitrile (25 ml) was stirred for 24 hours at room temperature. Acetonitrile was removed under vacuum to leave a residual liquid product which was flash chromatographed (25% ethyl acetate in petroleum ether) to yield a white solid as the desired product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06476053B1 |
| 출처 데이터셋 | uspto-grants-2002_11 |
| ORD ID | ord-2aed532edae34e4cb59d532c90c4e534 |
| 출처 메모 | uspto-grants-2002_11 |