HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 512824, compound → HCID 512842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 512824 | HCID 512824 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 512842 | HCID 512842 | — |
Reaction Steps
10% Palladium on carbon catalyst (5 wt %) was added to a stirred solution of N-nonyl citraconimide (0.02 M) prepared as described in Example 5 above in methanol (100 ml). Hydrogen gas was bubbled through this solution for three hours. The solution was then filtered over celite and concentrated in vacuo. Chromatography over silica gel gave the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06476053B1 |
| Source dataset | uspto-grants-2002_11 |
| ORD ID | ord-45cdda42417148d89a504e99b7aa8a56 |
| Source note | uspto-grants-2002_11 |